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Summer

...

2008

...

Research

Objectives

The purpose of this experiment was to determine the feasibility of improving sedimentation in the current AguaClara technology. The goal is to consistently produce effluent water with an effluent turbidity of less than 1 NTU. Currently, the AguaClara technology makes use of lamella, spaced apart by a distance on the order of 5 cm, in its sedimentation tanks. This study sought to determine the feasibility of significantly decreasing the spacing between plate settlers to create a filter-like media and create less than 1 NTU water. A set up was developed to collect turbidity data for a range of filter-like media spacing, to help determine the optimal spacing. To determine if filter-like media in place of lamella is practical in the sedimentation tank, the frequency in which clogging occurs was also noted. In addition, a cleaning method needed to be devised to ensure proper maintenance. This is because the AguaClara technology makes no use of electricity, and so the "filter media" needs to be able to be cleaned without the pumping water back up to backwash.

Methods

The set-up and method was similar to the CEE 453 project from Spring 2008.

Schematic

Image Added
Schematic of Apparatus Setup

As seen in the above schematic, a lab bench scale sedimentation and flocculator set-up was assembled for the experiment. The raw water, kaolin clay mixed with tap water, was mixed with a aluminum sulfate at dosage of 45 mg/L. This water was then pumped into the tube flocculator. The end of the flocculator flows into the sedimentation tank at a flow rate of 272 mL/min. The tube enters the from the top of the sedimentation tanks, passes through the straws to the bottom of the sedimentation tank, allowing the water to flow upward uniformly. The outlet above the straws draws the "clean water" out of the tank and into a turbidity meter.

Design Parameters

Wiki Markup


h2. Objectives


The purpose of this experiment was to determine the feasibility of improving sedimentation in the current AguaClara technology. The goal is to consistently produce effluent water with an effluent turbidity of less than 1 NTU. Currently, the AguaClara technology makes use of lamella, spaced apart by a distance on the order of 5 cm, in its sedimentation tanks. This study sought to determine the feasibility of significantly decreasing the spacing between plate settlers to create a filter-like media and create less than 1 NTU water. A set up was developed to collect turbidity data for a range of filter-like media spacing, to help determine the optimal spacing. To determine if filter-like media in place of lamella is practical in the sedimentation tank, the frequency in which clogging occurs was also noted. In addition, a cleaning method needed to be devised to ensure proper maintenance. This is because the AguaClara technology makes no use of electricity, and so the "filter media" needs to be able to be cleaned without the pumping water back up to backwash.



h2. Methods


The set-up and method was similar to the CEE 453 project from Spring 2008.

h3. Schematic

!schematic.png|height=300px!
*Schematic of Apparatus Setup*

As seen in the above schematic, a lab bench scale sedimentation and flocculator set-up was assembled for the experiment. The raw water, kaolin clay mixed with tap water, was mixed with a aluminum sulfate at dosage of 45 mg/L. This water was then pumped into the tube flocculator. The end of the flocculator flows into the sedimentation tank at a flow rate of 272 mL/min. The tube enters the from the top of the sedimentation tanks, passes through the straws to the bottom of the sedimentation tank, allowing the water to flow upward uniformly. The outlet above the straws draws the "clean water" out of the tank and into a turbidity meter.

h3. Design Parameters

{float:left|border=2px solid black}
!param.png|width=600px!
*Table 1:* Design parameters used in the old(initial) and new apparatus setup.
{float}
\\


The

...

table

...

above

...

contains

...

information

...

in

...

regards

...

to

...

the

...

tube

...

flocculator

...

inner

...

diameters

...

(d),

...

velocity

...

gradients

...

(G),

...

residence

...

times

...

(Ѳ),

...

flow

...

rates

...

(Q),

...

and

...

other

...

important

...

parameters

...

used

...

in

...

the

...

old

...

and

...

new

...

apparatus

...

setups

...

for

...

the

...

sedimentation

...

prototype.

...

For

...

both

...

setups

...

an

...

Alum

...

dosage

...

of

...

45

...

mg/L

...

was

...

used.

...

Additionally,

...

parameter

...

values

...

were

...

based

...

on

...

a

...

flocculator

...

length

...

of

...

10

...

meters

...

and

...

a

...

sedimentation

...

tank

...

angle

...

of

...

60

...

degrees.

...

It

...

is

...

important

...

to

...

note

...

that

...

the

...

value

...

for

...

the

...

velocity

...

gradient

...

G

...

must

...

be

...

5000/s

...

at

...

minimum

...

for

...

AguaClara

...

plants

...

and

...

in

...

both

...

setups

...

the

...

G

...

calculated

...

is

...

above

...

5000.

...

Also,

...

the

...

V

...

up values

...

for

...

both

...

setups

...

do

...

not

...

exceed

...

the

...

70

...

m/day

...

maximum

...

for

...

AguaClara

...

plants.


Initial Apparatus Setup

Wiki Markup
{float:

\\

h3. Initial Apparatus Setup

{float:left|border=2px solid black}
!IMG_0087.jpg|thumbnail!
*Initial Apparatus Setup*
{float}
\\


The

...

initial

...

apparatus

...

set

...

up

...

was

...

run

...

by

...

Process

...

Controller

...

which

...

had

...

functions

...

set

...

in

...

place

...

for

...

when

...

the

...

system

...

would

...

turn

...

on,

...

off,

...

or

...

drain.

...

It

...

also

...

included

...

a

...

pressure

...

sensor

...

that

...

would

...

control

...

the

...

flow

...

rate

...

of

...

the

...

system.

...

It

...

was

...

found

...

that

...

the

...

pressure

...

sensor

...

was

...

unreliable

...

and

...

sensitive

...

to

...

changes

...

in

...

the

...

environment.

...

Additionally,

...

the

...

flocculator

...

for

...

this

...

setup

...

led

...

to

...

a

...

high

...

velocity

...

gradient

...

(G)

...

of

...

129.1/s,

...

which

...

is

...

much

...

higher

...

than

...

the

...

desired

...

G

...

of

...

20

...

/s.

...

This

...

led

...

to

...

the

...

formation

...

of

...

very

...

small

...

flocs.

New Apparatus Setup

Wiki Markup

\\

h3. New Apparatus Setup

{float:left|border=2px solid black}
!IMG_0092.jpg|thumbnail!
*New Apparatus Setup*
{float}
\\


In

...

the

...

New

...

Apparatus

...

Setup

...

the

...

diameter

...

of

...

the

...

flocculator

...

was

...

increased.

...

This

...

allowed

...

for

...

an

...

increase

...

in

...

floc

...

size

...

and

...

a

...

significantly

...

lower

...

velocity

...

gradient

...

(G)

...

of

...

35.7/s.

...

Ideally,

...

a

...

G

...

around

...

20/s

...

is

...

wanted,

...

however,

...

such

...

a

...

velocity

...

gradient

...

may

...

have

...

caused

...

other

...

important

...

parameters

...

to

...

be

...

too

...

low.

...

Additionally,

...

the

...

flow

...

control

...

system

...

was

...

changed

...

to

...

utilize

...

a

...

peristaltic

...

pump

...

allowing

...

for

...

a

...

more

...

stable

...

system.

Equations

The following equations were used to determine critical settling velocity of each straws type, the velocity gradient of the flocculator, and the residence time of the flocculator.
Critical Settling Velocity
Image Added
Velocity Gradient
Image Added
Residence Time
Image Added

Length and Diameter Values

Wiki Markup


h3. Equations

The following equations were used to determine critical settling velocity of each straws type, the velocity gradient of the flocculator, and the residence time of the flocculator.
+Critical Settling Velocity+
!vc.png|height=50px!
+Velocity Gradient+
!G.png|height=50px!
+Residence Time+
!Theta.png|height=50px!

h3. Length and Diameter Values

{float:left|border=2px solid black}
!LDTable.png|width=600px!
*Table 2:* The data above shows length(L), diameter(D), and ratio of L/D values for each straw setup.
*The straw length was doubled because two straw packs were used in the sedimentation tank.
{float}
\\


In

...

regards

...

to

...

the

...

length

...

and

...

diameter

...

values,

...

the

...

table

...

above

...

shows

...

a

...

wide

...

spread

...

of

...

L/D

...

values.

...

The

...

no

...

straws

...

situation

...

uses

...

the

...

measurements

...

of

...

the

...

sedimentation

...

tank.

...

Additionally,

...

in

...

the

...

case

...

of

...

the

...

type

...

3

...

straw

...

situation,

...

the

...

length

...

of

...

the

...

3mm

...

diameter

...

straws

...

were

...

significantly

...

smaller

...

than

...

the

...

other

...

straws.

...

To

...

solve

...

this

...

issue,

...

two

...

packets

...

of

...

straws

...

were

...

used

...

in

...

the

...

sedimentation

...

tank

...

so

...

that

...

the

...

length

...

for

...

the

...

3mm

...

straws could be doubled.

Critical Settling Velocity Values

Wiki Markup
 could be doubled.
\\

h3. Critical Settling Velocity Values

{float:left|border=2px solid black}
!VCTable.png|width=600px!
*Table 3:* The data above shows the critical settling velocities of each straw setup
{float}
\\


Critical

...

settling

...

velocities

...

demonstrate

...

the

...

shortest

...

amount

...

of

...

time

...

it

...

takes

...

for

...

a

...

particle

...

to

...

settle

...

out.

...

The

...

V

...

c values

...

above

...

show

...

how

...

long

...

it

...

takes

...

for

...

particles

...

to

...

settle

...

out

...

in

...

each

...

straw

...

setup

...

situation.

...

In

...

comparison

...

to

...

the

...

AguaClara

...

plants

...

which

...

have

...

a

...

maximum

...

critical

...

velocity

...

of

...

10

...

m/day,

...

only

...

the

...

no

...

straws

...

situation

...

exceeds

...

this

...

value.

Straw Bundles

Wiki Markup

\\

h3. Straw Bundles

{float:left|border=2px solid black}
!IMG_0230.jpg|thumbnail!
*Type 1 Straws - 12mm*
{float}}
Wiki Markup

{float:left|border=2px solid black}
!medstraw.jpg|thumbnail!
*Type 2 Straws - 5mm*
{float}
Wiki Markup
{float:left|border=2px solid black}
!IMG_0227.jpg|thumbnail!
*Type 3 Straws - 3mm*
{float}
\\


For

...

the

...

initial

...

straw

...

setup,

...

each

...

straw

...

bundle

...

used

...

one

...

12mm

...

straw

...

a

...

tube

...

for

...

the

...

inlet

...

tube

...

of

...

the

...

flocculator

...

to

...

pass

...

through.

...

However,

...

when

...

the

...

straw

...

set

...

up

...

changed,

...

the

...

outer

...

diameter

...

of

...

the

...

flocculator

...

exceeded

...

12mm.

...

Therefore,

...

a

...

9/16ths

...

inch

...

inner

...

diameter

...

tube

...

was

...

ordered

...

to

...

accommodate

...

the

...

1/2

...

inch

...

outer

...

diameter

...

tube

...

used

...

in

...

the

...

new

...

straw

...

setup.

Results and Discussion

Matrix of Experiments

Wiki Markup



h2. Results and Discussion



h3. Matrix of Experiments

{float:left|border=2px solid black}
!matrix.png|width=600px!
*Table 4:* The data above is a matrix of the experiments performed for the Sedimentation Prototype.
{float}
\\


As

...

shown

...

by

...

the

...

table

...

above,

...

8

...

experiments

...

total

...

were

...

planned,

...

however

...

the

...

tests

...

on

...

the

...

type

...

3

...

straws

...

have

...

not

...

yet

...

been

...

completed.

...

At

...

this

...

point,

...

tests

...

have

...

only

...

been

...

performed

...

on

...

the

...

12

...

mm

...

and

...

5

...

mm

...

diameter

...

straws.

...

Three

...

trials

...

were

...

run

...

on

...

the

...

two

...

types

...

with

...

and

...

without

...

a

...

floc

...

blanket.

...

Due

...

to

...

some

...

problems

...

with

...

the

...

system

...

there

...

was

...

a

...

limited

...

about

...

of

...

useful

...

data.

...

Experiment Obstacles

Maintaining a floc blanket

While testing with the floc blanket it became clear that there was a problem with flocs settling out, decreasing the volume of the active suspended sludge. As seen in the image below, much of the sludge would settle along the incline of the settling column. This limited the effectiveness of the floc blanket, particularly in the trials with the 5 mm diameter straws.

Wiki Markup
 Obstacles


h5. Maintaining a floc blanket

While testing with the floc blanket it became clear that there was a problem with flocs settling out, decreasing the volume of the active suspended sludge. As seen in the image below, much of the sludge would settle along the incline of the settling column. This limited the effectiveness of the floc blanket, particularly in the trials with the 5 mm diameter straws.
{float:left|border=2px solid black}
!floc.jpg|thumbnail!
*Floc Blanket*
{float}
\\

h5. Turbidity meter readings

The horizontal tube connected to outlet of the settling column was tilted upwards which cause a sort of siphoning effect. The tube would fill with water and then empty, creating an intermediate flow of water into the turbidity meter. This created large and frequent jumps in the turbidity meter readings. A large portion of the data collected with this problem is difficult to read.

h5. Clogged Straws

In the 5 mm diameter experiments the straws clogged. This occurred within 15 hours of the final trail without a floc blanket. Once clogged flocs being pumped into the system would push the flocs settled out in the straws to the top, create a floc formation on top of the straws, as seen above. Particles would eventually float off the top of the floc blanket that formed on top increasing the turbidity of the effluent water.


Turbidity meter readings

The horizontal tube connected to outlet of the settling column was tilted upwards which cause a sort of siphoning effect. The tube would fill with water and then empty, creating an intermediate flow of water into the turbidity meter. This created large and frequent jumps in the turbidity meter readings. A large portion of the data collected with this problem is difficult to read.

Clogged Straws

In the 5 mm diameter experiments the straws clogged. This occurred within 15 hours of the final trail without a floc blanket. Once clogged flocs being pumped into the system would push the flocs settled out in the straws to the top, create a floc formation on top of the straws, as seen above. Particles would eventually float off the top of the floc blanket that formed on top increasing the turbidity of the effluent water.

Wiki Markup
{float:left|border=2px solid black}
!clog.jpg|thumbnail!
*Clogged Straws*
{float}
\\

h3. Experimental Trials


h5. No straw trials.

It is important to first note that the raw water turbidity during this test was around 200 NTU. The effluent turbidity remained between 30 and 20 NTU, and the average percent removal was around 86.4%.

!graph1.png|width=800px!\\

h5. Type 1 Straw Trials

!graph2.png|width=800px!

 This trial for the largest diameter straws (12 mm) maintained a steady effluent turbidity of 15 NTU. The average percent removal for this trial was 82%.



!graph3.png|width=800px!\\
The effluent turbidity with the floc blanket was much less stable for the first 20 hours. After the 25th hour the effluent turbidity remained around 9 NTU. The Average percent removal was 90%.



h5. Type 2 Straw Trials

!graph4.png|width=800px!

—The type 2 straws yielded an effluent turbidity of around 12 NTU until around the 11th hour. The increase in turbidity could have occurred due to the clogging of the straws. The average percent removal for this trial was 86%.


!graph5.png|width=800px!

     As mentioned before the turbidity meter readings for some of the data was jumpy.  Not unlike the 12 mm diameter straw trials, the 5 mm trial performed better with a floc blanket than with out. The effluent turbidity of this trial remained around 8 NTU. The percent removal for this trial was 91%. 


h2.Conclusions


From the limited available data it can be determined that straws perform significantly better than the settling column tube. There is a slight trend of lowering turbidities as the critical velocities of the system decreasing, which was expected. The combination of the floc blanket and lower Vc values seem to produce the most favorables results of lower effluent turbidity readings. Due the problems with maintaining floc blankets, more testing should be done to determine the effectiveness of the floc blankets.

The clogging of the straws indicates better removal of particles from the water. The particles are being removed from the water despite the higher turbidity readings. This may be due to the significantly lower critical velocities found in the smaller straws. The effluent turbidities in all of the experiments, however, were unfavorable. Improving the flocculator and the overall experimental setup may help to produce lower effluent turbidities.



h2.Future Work

In terms of the immediate future (the last few weeks of summer), testing will continue on the type 3 straws. One of the major improvements to the experimental set will be the improvement of flocculation by lengthening flocculator, thus increasing GѲ. Another improvement to the flocculation will be increasing the number of changes in flow within the flocculation, hopefully creating my collision of particles and increasing floc size. To solve the problem of the straws clogging a lower alum dosage of around 25 mg/L will be used instead of the 45 mg/L. Additional tests will be conducted without the use of a floc blanket, due to difficulties with maintaining a stable floc blanket in the previous tests. Future work may include the use of floc blankets since they do contribute to lower effluent turbidity values.

It may be beneficial to examine the head lose through the straws given laminar flow. The Hagen-Poiseuille equation can be used to find the head loss.

To determine the feasibility of implementing these changes in the sedimentation tanks in Honduras, research must be done on the availability of materials with similar geometry. This material could be purchased and tested in the pilot plant set up at the Cornell Water Treatment Plant.


Experimental Trials

No straw trials.

It is important to first note that the raw water turbidity during this test was around 200 NTU. The effluent turbidity remained between 30 and 20 NTU, and the average percent removal was around 86.4%.

Image Added

Type 1 Straw Trials

Image Added

 This trial for the largest diameter straws (12 mm) maintained a steady effluent turbidity of 15 NTU. The average percent removal for this trial was 82%.

Image Added
The effluent turbidity with the floc blanket was much less stable for the first 20 hours. After the 25th hour the effluent turbidity remained around 9 NTU. The Average percent removal was 90%.

Type 2 Straw Trials

Image Added

—The type 2 straws yielded an effluent turbidity of around 12 NTU until around the 11th hour. The increase in turbidity could have occurred due to the clogging of the straws. The average percent removal for this trial was 86%.

Image Added

     As mentioned before the turbidity meter readings for some of the data was jumpy.  Not unlike the 12 mm diameter straw trials, the 5 mm trial performed better with a floc blanket than with out. The effluent turbidity of this trial remained around 8 NTU. The percent removal for this trial was 91%. 

Conclusions

From the limited available data it can be determined that straws perform significantly better than the settling column tube. There is a slight trend of lowering turbidities as the critical velocities of the system decreasing, which was expected. The combination of the floc blanket and lower Vc values seem to produce the most favorables results of lower effluent turbidity readings. Due the problems with maintaining floc blankets, more testing should be done to determine the effectiveness of the floc blankets.

The clogging of the straws indicates better removal of particles from the water. The particles are being removed from the water despite the higher turbidity readings. This may be due to the significantly lower critical velocities found in the smaller straws. The effluent turbidities in all of the experiments, however, were unfavorable. Improving the flocculator and the overall experimental setup may help to produce lower effluent turbidities.

Future Work

In terms of the immediate future (the last few weeks of summer), testing will continue on the type 3 straws. One of the major improvements to the experimental set will be the improvement of flocculation by lengthening flocculator, thus increasing GѲ. Another improvement to the flocculation will be increasing the number of changes in flow within the flocculation, hopefully creating my collision of particles and increasing floc size. To solve the problem of the straws clogging a lower alum dosage of around 25 mg/L will be used instead of the 45 mg/L. Additional tests will be conducted without the use of a floc blanket, due to difficulties with maintaining a stable floc blanket in the previous tests. Future work may include the use of floc blankets since they do contribute to lower effluent turbidity values.

It may be beneficial to examine the head lose through the straws given laminar flow. The Hagen-Poiseuille equation can be used to find the head loss.

To determine the feasibility of implementing these changes in the sedimentation tanks in Honduras, research must be done on the availability of materials with similar geometry. This material could be purchased and tested in the pilot plant set up at the Cornell Water Treatment Plant.