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The experiment lasted approximately 12.5 hours for A2 and 16.5 hours for A1. Both failed and then leveled off. Neither apparatus reached the saturation point for lime (pH = 12.6), with A1 reaching 12.3 and A2 reaching 11.6 as the peak pHs. However, it is important to note that this experiment was conducted before new pH probes were purchased and implemented.
Visually, it was noted that while the lime remained primarily in the vertical column of A2, it traveled up into the diagonal column of A1 sometimes filling 80% of the column. For both apparatuses, it was discovered that a significant amount of lime was getting caught in the elbows---despite blending the slurry and keeping a low upflow velocity. From observing the experiment after failure, the team also noted that there may be preferential flow paths through the settled lime slurry and this may result in the relatively quick failure (despite having such a large amount of lime).
After this experiment, the team hypothesized that pulsing in a lime slurry could allow the experiments to run for longer than 12 or 16 hours and reach the desired goal of 24 hours.
Figure 1 - Experiment 6
This experiment was conducted to test the effect of blending the lime slurry to observe how smaller particles act in the two apparatuses.